ISO 100, F1.8, Shutter at 1/200, using a printable focus chart about 1 meter away from the camera.
That seems to be too close. Canon recommends 50x focal length, which would be about 12' away with the 85mm ... ~ 4 meters, if I did the math correctly.
I suppose if your primary use for the 85mm is head+shoulders portraits, that might justify doing the AF-MA at that specific distance.
It appears from your later post that you got the 85mm AF-MA to work. Great! For those who are struggling to get Auto-Dot-Tune to behave, it would probably be a good thing to start at 50x distance. Once it is working, then and only then use something other than 50x.
The 85mm f1.2L would certainly be a lens that would benefit from AF-MA, with its very shallow DOF.
It would be interesting to see what the setting for it would be at 1', 3', 8', 12', 50', and infinity.
FWIW: My speculation is that the newer Sigma lenses with their "Dock" allow AF-MA at different distances. I am unclear how that would integrate with a Canon body however.